Samsung RT34M Bedienungsanleitung PDF herunterladen (Seite 23)

Dushyant Patel Review of Literature

S.K.P.C.P.E.R., Kherva 11 M .Pharm. Thesis

13. Determination of gabapentin in

human plasma and urine by high-

performance liquid chromatography

with UV-vis detection

HPLC Extraction method: SPE C18

cartridge

Derivatization reagent: 1,2-

naphthoquinone-4-sulphonic

acid sodium salt (NQS)

Column: C18

MP: ACN:10mM OPA

(pH 2.5,v/v)

IS: Baclofen

14. Sensitive high-performance liquid

chromatographic quantitation of

gabapentin in human serum using

liquid-liquid extraction and pre-

column derivatization with 9-

fluorenylmethyl chloroformate

HPLC Extraction method: LLE

Extracting solvent:

dichloromethane : 2 propanol

(1:1, v/v)

Derivatization reagent: 9-

fluorenyl methyl chloroformate

(FMOC-Cl)

Column: Shimpack CLC-C18

(150 mm x 4.6 mm)

MP: methanol:0.05 M sodium

phosphate buffer (73:27, v/v;

pH of 3.9) containing 1 ml/l

triethylamine

15. Simple and sensitive liquid

chromatographic method with

fluorimetric detection for the

analysis of gabapentin in human

plasma

HPLC Derivatization reagent: (2-

naphthoxy)acetyl chloride

(NAC)

Column: phenyl-hexyl column

MP: sodium acetate buffer

(100 mM; pH 5.0):methanol

(32:68, v/v)

Detection method:

Fluorimetry

(EX: 225 nm, EM: 360 nm)

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