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Dushyant Patel LC-MS/MS Method

S.K.P.C.P.E.R., Kherva 58 M .Pharm. Thesis

¾ The % CV Extracted for LQC, MQC and HQC samples of GBP were 1.69, 2.20 and

1.95, respectively. (Table No. 4.17).

¾ The % CV of recovery across QC level for GBP was 0.64 (Table No. 4.18).

¾ The % CV within LEV IS concentration of Unextracted and Extracted sample area

across QC level was 1.92 and 2.65, respectively (Table No.4.19).

TABLE NO: 4.17 TABLE NO: 4.18

RECOVERY OF GBP VARIABILITY ACROSS

QC LEVELS OF GBP

Sr. No.

LQC (0.15 µg/ml)

Area of GBP

QC LEVELS %Recovery

LQC 75.16

Unextracted Extracted

MQC 74.24

1 875947 684127 HQC 74.48

2 899832 667856 Mean 74.63

3 904803 676503 SD 0.476

4 889850 662878 %CV 0.64

5 877122 659813

6 880627 653359

n 6 6

Mean 888030.17 667422.67

SD 12196.07 11296.22

%CV 1.37 1.69

%Recovery 75.16

Sr. No.

MQC (2.00 µg/ml)

Area of GBP

Unextracted Extracted

1 11855128 8942349

2 12044387 9307512

3 12039162 8913235

4 12160617 8900607

5 12026886 8741100

6 12092220 8811499

n 6 6

Mean 12036400.00 8936050.33

SD 101555.12 196631.07

%CV 0.84 2.20

%Recovery 74.24

Sr. No.

HQC (4.50 µg/ml)

Area of GBP

Unextracted Extracted

1 25943141 18948482

2 26361578 19188069

3 26357843 19070589

4 25786432 20011910

5 25622017 19249242

6 25534676 19421973

n 6 6

Mean 25934281.17 19315044.17

SD 358083.31 377262.38

%CV 1.38 1.95

%Recovery 74.48

1 2 ... 65 66 67 68 69 70 71 72 73 74 75 ... 92 93

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